COURSE OBJECTIVES
1. To provides fundamental pharmaceutical methods of analysis applied in all pharmaceutical analytical laboratories.
2. To learn about various spectroscopic and chromatographic techniques for the characterization and separation of pharmaceutically important chemical compounds.
3. To understand and interpret the spectral analysis.
COURSE LEARNING OUTCOMES (CLO)
CLO: 1. To provides fundamental pharmaceutical methods of analysis applied in all pharmaceutical analytical laboratories.
CLO: 2. Perform spectroscopic and chromatographic techniques for the characterization and separation of pharmaceutical compounds.
CLO: 3. Analyze the spectrum and chromatogram of unknown chemical compounds.
COURSE CONTENTS
1. Laboratory protocols
2. Standardization of NaOH by using oxalic acid
3. Standardization of HCl by using sodium carbonate
4. Verification of Beer’s Lambert law
5. Determination of λ max of given FeCl3 solution
6. Preparation of standard curve of K2Cr2O7 with different concentration
7. Determination of percentage purity of given sample Ciprofloxacin infusion by using UV/visible spectrophotometer
8. Determination of percentage purity of given sample of paracetamol tablets by UV spectrophotometer
9. Determination of percentage purity of given sample of Chlorpheniramine tablets by using UV/visible spectrophotometer
10. To separate the sample of un-known mixture by using thin layer chromatography
11. To determine the viscosity of the given sample (liquids)using brook field viscometer
12. To find out the refractive index of the given sample (liquid) using Abbe’s refractometer
13. To find out the unknown composition of given mixtures using Abbe’s refractometer